| 1. Identity statement | ||||
| Reference Type | Journal Article | |||
| Site | mtc-m21b.sid.inpe.br | |||
| Holder Code | isadg {BR SPINPE} ibi 8JMKD3MGPCW/3DT298S | |||
| Identifier | 8JMKD3MGP3W34P/3KBFBN5 | |||
| Repository | sid.inpe.br/mtc-m21b/2015/09.30.17.11 (restricted access) | |||
| Last Update | 2015:10.02.11.36.01 (UTC) administrator | |||
| Metadata Repository | sid.inpe.br/mtc-m21b/2015/09.30.17.11.40 | |||
| Metadata Last Update | 2022:08.22.23.17.04 (UTC) administrator | |||
| DOI | 10.1016/j.snb.2015.04.085 | |||
| ISSN | 0250-6874 | |||
| Citation Key | SilvaZanVicCorFat:2015:ElDeRo | |||
| Title | Electrochemical determination of rosuvastatin calcium in pharmaceutical and human body fluid samples using a composite of vertically aligned carbon nanotubes and graphene oxide as the electrode material  | |||
| Year | 2015 | |||
| Month | May | |||
| Access Date | 2024, May 19 | |||
| Type of Work | journal article | |||
| Secondary Type | PRE PI | |||
| Number of Files | 1 | |||
| Size | 1937 KiB | |||
| 2. Context | ||||
| Author | 1 Silva, Tiago Almeida 2 Zanin, Hudson G. 3 Vicentini, Fernando Campanha 4 Corat, Evaldo José 5 Fatibello Filho, Orlando | |||
| Resume Identifier | 1 2 3 4 8JMKD3MGP5W/3C9JH33 | |||
| Group | 1 2 3 4 LAS-CTE-INPE-MCTI-GOV-BR | |||
| Affiliation | 1 Universidade Federal de São Carlos (UFSCar) 2 Universidade do Vale do Paraíba (UNIVAP) 3 Universidade Federal de São Carlos (UFSCar) 4 Instituto Nacional de Pesquisas Espaciais (INPE) 5 Universidade Federal de São Carlos (UFSCar) | |||
| Author e-Mail Address | 1 2 3 4 evaldo.corat@inpe.br 5 bello@ufscar.br | |||
| Journal | Sensors and Actuators B: Chemical | |||
| Volume | 218 | |||
| History (UTC) | 2015-09-30 17:11:40 :: simone -> administrator :: 2021-07-28 21:31:49 :: administrator -> simone :: 2015 2022-03-11 17:28:08 :: simone -> administrator :: 2015 2022-03-11 18:04:59 :: administrator -> simone :: 2015 2022-03-14 12:34:22 :: simone -> administrator :: 2015 2022-08-22 23:17:04 :: administrator -> simone :: 2015 | |||
| 3. Content and structure | ||||
| Is the master or a copy? | is the master | |||
| Content Stage | completed | |||
| Transferable | 1 | |||
| Content Type | External Contribution | |||
| Version Type | publisher | |||
| Keywords | Biological samples Carbon-carbon composite Graphene oxide Pharmaceutical samples Rosuvastatin calcium Vertically aligned carbon nanotubes | |||
| Abstract | A novel electrochemical method for the determination of rosuvastatin calcium (RC) using a composite of vertically aligned carbon nanotubes and graphene oxide (VACNT-GO) as the electrode material is proposed. The VACNT-GO electrode was synthesized using a microwave-assisted chemical vapor deposition method followed by oxygen plasma treatment. The VACNT-GO electrode presented superhydrophilic behavior and fast charge transfer, which are very attractive for electrochemical applications. The RC molecule presented an oxidation process at +1.26 V vs. Ag/AgCl (3.0 mol L-1 KCl) in phosphate buffer solution (pH 2), and this redox behavior was explored for its voltammetric determination. Using square-wave adsorptive anodic stripping voltammetry (SWAdASV) under optimized conditions, the analytical curve was linear in RC concentration range from 0.48 to 46.72 μmol L-1 with a limit of detection of 0.06 μmol L-1. The developed SWAdASV method was applied for RC quantification in commercial pharmaceutical samples, and the results are consistent with those obtained by the comparative spectrophotometric method at a confidence level of 95%. Moreover, RC was determined in human body fluid samples of urine and human serum. | |||
| Area | FISMAT | |||
| Arrangement | urlib.net > LABAS > Electrochemical determination of... | |||
| doc Directory Content | access | |||
| source Directory Content | there are no files | |||
| agreement Directory Content |
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| 4. Conditions of access and use | ||||
| Language | en | |||
| Target File | silva_electrochemical.pdf | |||
| User Group | simone | |||
| Reader Group | administrator simone | |||
| Visibility | shown | |||
| Archiving Policy | denypublisher denyfinaldraft24 | |||
| Read Permission | deny from all and allow from 150.163 | |||
| Update Permission | not transferred | |||
| 5. Allied materials | ||||
| Mirror Repository | urlib.net/www/2011/03.29.20.55 | |||
| Next Higher Units | 8JMKD3MGPCW/3ESR3H2 | |||
| Citing Item List | sid.inpe.br/bibdigital/2013/09.24.19.30 1 | |||
| Dissemination | WEBSCI; PORTALCAPES. | |||
| Host Collection | sid.inpe.br/mtc-m21b/2013/09.26.14.25.20 | |||
| 6. Notes | ||||
| Empty Fields | alternatejournal archivist callnumber copyholder copyright creatorhistory descriptionlevel e-mailaddress format isbn label lineage mark nextedition notes number orcid pages parameterlist parentrepositories previousedition previouslowerunit progress project rightsholder schedulinginformation secondarydate secondarykey secondarymark session shorttitle sponsor subject tertiarymark tertiarytype url | |||
| 7. Description control | ||||
| e-Mail (login) | simone | |||
| update | ||||